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A solid of a uniform cross-section of right-angled isosceles triangles perpendicular to the $x$-axis has a base $x^2 + y^2 = 16$. Solve for the volume.

Let $\theta$ be the angle between the $x$-axis and the radii of a circle for $0 \leq \theta \leq \frac{\pi}{2}$. The hypotenuse of the right-angled triangles is $8\sin \theta$. As the relation between a hypotenuse and area of a right-angled isosceles triangle is $\frac{\text{Hyp}^2}{4}$, the area of a single triangle is $16\sin^2 \theta$. As the solid is symmetric, we integrate over the domain and multiply the answer by 2.

\begin{align*} &\quad\quad 2\int_0^\frac{\pi}{2}16\sin^2 \theta \quad d\theta\\ &= 32\int_0^\frac{\pi}{2}\frac{1}{2}-\frac{1}{2}\cos 2\theta \quad d\theta\\ &=32\left[\frac{1}{2}\theta - \frac{1}{4}\sin 2\theta \right]_0^\frac{\pi}{2}\\ &= 8\pi \end{align*}

However, this answer is incorrect as when one uses the more conventional method to solve:

Let the hypotenuse of one of the triangles be $2y$. Then the area is $y^2$. \begin{align*} Volume &= \int_{-4}^4y^2dx\\ &= \int_{-4}^416-x^2dx\\ &= \left[16x-\frac{1}{3}x^3\right]_{-4}^4\\ &= \frac{256}{3} \end{align*}

which appears to be the correct answer. I'm curious as to why my alternative method doesn't work.

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Using a cartesian coordinate system, we have (as you pointed out in your question):

\begin{equation} V = \int_{a}^{b} A(x) dx = \int_{-4}^{4} \frac{(\sqrt2y)(\sqrt2y)}{2} dx = \int_{-4}^{4} y^2 dx = \int_{-4}^{4} 16-x^2 dx = \frac{256}{3} \end{equation}

Now if you want to use polar coordinates (where $ \theta $ is the angle between the $ x $ axis and the radius of the circle), you should proceed as follows:

\begin{equation} V = \int_{a}^{b} A(x) dx = \int_{-4}^{4} y^2 dx \end{equation}

Since $ y = 4sin(\theta) $ and $ x = 4cos(\theta) \rightarrow dx = -4sin(\theta)d\theta $, we get:

\begin{equation} \int_{cos^{-1}\big(\frac{-4}{4}\big)}^{cos^{-1}\big(\frac{4}{4}\big)} (4sin(\theta))^2 (-4sin(\theta))d\theta = -4^3 \int_{\pi}^{0} sin^3(\theta) d\theta = 4^3 \int_{0}^{\pi} sin^3(\theta) d\theta = \frac{256}{3} \end{equation}